1 & 2. See course reader
3.
a) 134 peak | b. | c) 91 | d. |
e) M+1 peak which is 12C813C11H1016O1
4.
5. No. Trans-cinnamaldehyde was used and thus only trans,trans and the cis,trans isomers were possible. Appropriate structures needed for full credit.
6. The nitronium ion is a stronger electrophile. Experimental observations support this. Deactivated aryl compounds can by polynitrated. In general, aryl compounds cannot undergo polyacylation. Appropriate examples needed for full credit.
7. Water is a stronger base then nitric acid. Thus, the water is a better competitor for the proton from sulfuric acid preventing protonation of the nitric acid. Also, water is a product. Excess water would drive the reaction to the left.
8. | 9. |
10. Mesitylene
11 .